Gruner Group Publications

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Current list of publications available electronically (incomplete)
Joel T. Weiss, Katherine S. Shanks, Hugh T. Philipp, Julian Becker, Darol Chamberlain, Prafull Purohit, Mark W. Tate, Sol M. Gruner (2017). High Dynamic Range X-ray Detector Pixel Architectures Utilizing Charge Removal (IEEE Transactions in Nuclear Science,In Press). Prepublication version.
X. Nguyen, Prafull Purohit, Ajay Yadav, Mark W. Tate, Celesta S. Chang, Ramamoorthy Ramesh, Sol M. Gruner, David A. Muller (2016). Reconstruction of Polarization Vortices by Diffraction Mapping of Ferroelectric PbTiO3/SrTiO3 Superlattice Using a High Dynamic Range Pixelated Detector. Microscopy and Microanalysis, 22 (Suppl. 3): 472-473.
Kayla X. Nguyen, Prafull Purohit, Robert Hovden, Emrah Turgut, Mark W. Tate, Lena F. Kourkoutis, Gregory D. Fuchs, Sol M. Gruner, David A. Muller (2016). 4D-STEM for Quantitative Imaging of Magnetic Materials with Enhanced Contrast and Resolution. Microscopy and Microanalysis, 22 (Suppl. 3): 1718-1719. DOI: 10.1017/S1431927616009430
Julian Becker, Mark W. Tate, Katherine S. Shanks, Hugh T. Philipp, Joel T. Weiss, Prafull Purohit, Darol Chamberlain, Jacob P. C. Ruff and Sol M. Gruner (2016).  Characterization of CdTe Sensors with Schottky Contacts Coupled to Charge-Integrating Pixel Array Detectors for X-Ray Science. JINST 11: P12013. Preprint:  doi:10.1088/1748-0221/11/12/P12013
David A. Muller, Kayla X. Nguyen, Mark W. Tate, Prafull Purohit, Celesta Chang, Michael Cao and Sol M. Gruner (2016). An Electron Microscope Pixel Array Detector as a Universal STEM Detector. Microscopy and Microanalysis, 22 (Suppl. 3): 478-479. 10.1017/S143192761600324X
David A. Muller, Yimo Han, Kayla X. Nguyen, Mark W. Tate, Prafull Purohit, Saien Xie, Jiwoong Park and Sol M. Gruner (2016). Electron Diffraction from a Single Atom and Optimal Signal Detection. Microscopy and Microanalysis, 22 (Suppl. 3): 846-847. 10.1017/S1431927616005079
Chae Un Kim, HyoJin Song, Balendu Sankara Avvaru, Sol M. Gruner, Sang Youn Park and  Robert McKenna (2016).  Tracking solvent and protein movement during CO2 release in carbonic anhydrase II crystals. Proc. Natl. Acad. Sci. USA 113: 5257-5262 10.1073/pnas.1520786113
Rui-Qi Song, Tobias N. Hoheisel, Hiroaki Sai, Zihui Li, Joseph D. Carloni, Suntao Wang, Randall E. Youngman, Shefford P. Baker, Sol M. Gruner, Ulrich Wiesner, and Lara A. Estroff (2016). Formation of Periodically-Ordered Calcium Phosphate Nanostructures by Block Copolymer-Directed Self-Assembly. Chem. Mater. 28: 838-847. 10.1021/acs.chemmater.5b04266
Yao Sun, Hiroaki Sai, Katherine A. Spoth, Kwan Wee Tan, Ulrike Werner-Zwanziger, Josef Zwanziger, Sol M. Gruner, Lena F. Kourkoutis, and Ulrich Wiesner (2015). Stimuli-responsive shapeshifting mesoporous silica nanoparticles. Nano Letters. 16: 651-655. 10.1021/acs.nanolett.5b04395
Qingqiu Huang, Sol. M. Gruner, Chae Un Kim, Yuxin Mao, Xiaochun Wu, and Doletha M. E. Szebenyi. Reduction of lattice disorder in protein crystals by high pressure cryocooling (2016). J. Appl. Crystallography. 49:149-157.
Mark W. Tate, Prafull Purohit, Darol Chamberlain, Kayla X. Nguyen, Robert M. Hovden, Celesta S. Chang, Pratiti Deb, Emrah Turgut, John T. Heron, Darrell G. Schlom, Daniel C. Ralph, Gregory D. Fuchs, Katherine S. Shanks, Hugh T. Philipp, David A. Muller & Sol M. Gruner (2016). High dynamic range pixel array detector for scanning transmission electron microscopy. Microscopy & Microanalysis. 22: 237-249doi:10.1017/S1431927615015664
Hugh T. Philipp, Mark W. Tate, Prafull Purohit, Katherine S. Shanks, Joel T. Weiss and Sol M. Gruner (2016). High-speed x-ray imaging pixel array detector for synchrotron bunch isolation with frame rates up to 10 MHz. J. Synchrotron Radiation. 23: 395-403.
Spencer W. Robbins, Peter Beaucage, Hiroaki Sai, Kwan Wee Tan, Jorg G. Werner, James P. Sethna, Francis J. DiSalvo, Sol M. Gruner, Robert B. van Dover, Ulrich Wiesner (2016). Block copolymer self-assembly directed synthesis of mesoporous gyroid superconductors.Science Advances 21: e1501119. doi: 10.1126/sciadv.1501119.
K. X. Nguyen, R. Hovden, M. W. Tate, P. Purohit, J. Heron, C. Chang, S. M. Gruner, D. A. Muller (2015).  Lorentz-STEM imaging of Fields and Domains using a High-Speed, High-Dynamic Range Pixel Array Detector at Atomic Resolution. Microscopy & Microanalysis 21: 2309-2310 (Suppl. 3), Paper No. 1153. (link).
Jennifer Wierman, Ti-Yen Lan, Mark Tate, Hugh Philipp, Veit Elser and Sol Gruner (2016). Protein Crystal Structure from Non-oriented, Single-axis Sparse X-ray Data. IUCrJ 3:43-50 (link).
Hugh T. Philipp, Mark W. Tate, Prafull Purohit, Darol Chamberlain, Katherine S. Shanks, Joel T. Weiss and Sol M. Gruner. High-Speed X-ray Imaging with the Keck Pixel Array Detector (Keck PAD) for Time-Resolved Experiments at Synchrotron Sources (2016). AIP Conference Proceedings 1741: 040036. (pre-pub).
Katherine S. Shanks, Hugh T. Philipp, Joel T. Weiss, Julian Becker, Mark W. Tate and Sol M. Gruner. The High Dynamic Range Pixel Array Detector (HDR-PAD): Concept and Design (2016). AIP Conference Proceedings 1741: 040009. (pre-pub).
Chae Un Kim, Mark W. Tate, and Sol M. Gruner. Glass-to-cryogenic liquid transitions in water solutions examined by crack-healing (2015). Proc. Natl. Acad. Sci. USA 112:11765-11770. (link). (pdf).
Julian Becker, Mark W. Tate, Katherine S. Shanks, Hugh T. Philipp, Joel T. Weiss, Prafull Purohit, Darol Chamberlain and Sol M. Gruner. High-Speed Imaging at High X-ray Energy: CdTe Sensors Coupled to Charge-Integrating Pixel Array Detectors (2016). AIP Conference Proceedings 1741: 040037.  (pre-pub).
Joel T. Weiss, Julian Becker, Katherine S. Shanks, Hugh T. Philipp, Mark W. Tate and Sol M. Gruner. Potential Beneficial Effects of Electron-Hole Plasmas Created in Silicon Sensors by XFEL-Like High Intensity Pulses for Detector Development (2016). AIP Conference Proceedings 1741: 040038. (pre-pub).
Kwan Wee Tan, Hiroaki Sai, Spencer W. Robbins, Jörg G. Werner, Tobias N. Hoheisel, Sarah A. Hesse, Peter A. Beaucage, Francis J. DiSalvo, Sol M. Gruner, Martin Murtagh, Ulrich Wiesner. Ordered Mesoporous Crystalline Aluminas from Self‑Assembly of ABC Triblock Terpolymer–Butanol–Alumina Sols. RSC Advances 5 (2015) 49287-49294.(pdf) (link)
Morgan Stefik, Juho Song, Hiroaki Sai, Stefan Guldin, Patrick Boldrighini, M. Christopher Orilall, Ullrich Steiner, Sol M. Gruner, Ulrich Wiesner. Ordered mesoporous titania from highly amphiphilic block copolymers: tuned solution conditions enable highly ordered morphologies and ultra-large mesopores. J. Materials Chemistry A 3 (2015) 11478-11492.(pdf) (link)
Heinz Graafsma, Julian Becker, Sol M. Gruner. Integrating hybrid area detectors for storage ring and free-electron laser applications. In Synchrotron Light Sources and Free-Electron Lasers, E. Jaeschke, S. Khan, J.R. Schneider and J.B. Hastings, eds., (Springer, Heidelberg, Germany, 2015) (Book link).(link).
Sol M. Gruner. Expanding the femtosecond crystallographic toolkit (Invited commentary). Proc. Natl. Acad. Sci. USA 111 (2014) 16986-16987 (pdf) (link)
Sol M. Gruner & Eaton E. Lattman. Biostructural Science Inspired by Next Generation X-ray Sources. Annual Rev. Biophysics 44 (2015) 33-51. (link)
Kartik Ayyer, Hugh T. Philipp, Mark W. Tate, Jennifer L. Wierman, Veit Elser and Sol M. Gruner. Determination of crystallographic intensities from sparse data. IUCrJ 2 (2015) 29-34. (pdf) (link) . Serial crystallography for the masses? Commentary on paper by J.P. Wright (link).
Enju Lima, Yuriy Chushkin, Peter Van Der Linden, Federico Zontone, Philippe Carpentier, Petra Pernot, Chae Un Kim, and Sol M. Gruner. Cryo x-ray diffraction microscopy utilizing high-pressure cryopreservation. Phys. Rev. E, 90 (2014) 042713. (pdf) (link)
Alper Ercan, Mark W. Tate, Sol M. Gruner. A high frame rate x-ray image sensor. IEEE Sensors Journal 15 (2015) 1523-1531. (link).
Spencer W. Robbins, Hiroaki Sai, Francis J. DiSalvo, Sol M. Gruner, Ulrich Wiesner. Monolithic Gyroidal Mesoporous Mixed Titanium-Niobium Nitrides. ACS Nano. 8 (2014) 8217-8223. (link).
Michael Heymann, Achini Opthalage, Jennifer L. Wierman, Sathish Akella, Doletha M.E. Szebenyi, Sol M. Gruner & Seth Fraden (2014). Room-temperature serial crystallography using a kinetically optimized microfluidic device for protein crystallization and on-chip X-ray diffraction. IUCrJ 1 (2014)349-360. (pdf), (link).
P.K. Lambert, C.J. Hustedt, K.S. Vecchio, E.L. Huskins, D.T. Casem, S.M. Gruner, M.W. Tate, H.T. Philipp,  A.R. Woll, P. Purohit, J.T. Weiss, V. Kannan, K.T. Ramesh, P. Kenesei, J.S. Okasinski, J. Almer, M. Zhao, A.G. Ananiadis, and T.C. Hufnagel. Time-resolved x-ray diffraction techniques for bulk polycrystalline materials under dynamic loading. Rev. Sci. Instr. 85 (2014) 093901. (link). (pdf).
Klaus Giewekemeyer, Hugh T. Philipp, Robin N. Wilke, Andrew Aquila, Markus Osterhoff, Mark W. Tate, Katherine S. Shanks, Sol M. Gruner and Adrian P. Mancuso. High Dynamic Range Coherent Diffractive Imaging: Ptychography using the Mixed-Mode Pixel Array Detector. J. Synchrotron Radiation. 21 (2014) 1167-1174 (link) (pdf).
Kartik Ayyer, Hugh T. Philipp, Mark W. Tate, Veit Elser, Sol M. Gruner.  Real-space x-ray tomographic reconstruction of randomly oriented objects with sparse data frames. Optics Express. 22 (2014) 2403-2413 (doi: 10.1364/OE.22.002403).
Zihui Li, Kahyun Hur, Hiroaki Sai, Takeshi Higuchi, Atsushi Takahara, Hiroshi Jinnai, Sol M. Gruner and Ulrich Wiesner.  Linking experiment and theory for three-dimensional networked binary metal nanoparticle–triblock terpolymer superstructures. Nature Commun. 5 (2014) 3247 (doi: 10.1038/ncomms4247).
Zihui Li, Hiroaki Sai, Kwan Wee Tan, Tobias N. Hoheisel, Sol M. Gruner, and Ulrich Wiesner.  Ordered Nanostructured Ceramic-Metal Composites through Multifunctional Block Copolymer-Metal Nanoparticle Self-Assembly. J. Sol-Gel Science & Technology. Oct. 2013. (doi: 10.1007/s10971-013-3169-4).
Angela V. Toms, Anagha Deshpande, Randall McNally, Youngjee Jeong, Julia Rogers, Sol M. Gruner, Chae Un Kim, Scott Ficarro, Jarrod A. Marto, Martin Sattler, James D. Griffin and Michael J. Eck.  Structure of a pseudokinase domain switch that controls oncogenic activation of Jak kinases. Nature Structure & Molecular Biol. 20 (2013) 1221-1223 (link).
G.H. Hoffstaetter et al., Readiness for the Cornell ERL. Proc. of IPAC 2013, paper WEPWO061. (pdf).
Jennifer L.  Wierman, Jonathan S.  Alden, Chae Un Kim, Paul L.  McEuen and Sol M.  Gruner.  Graphene as protein crystal mounting material to reduce background scatter. J. Appl. Cryst. 46 (2013) 1501-1507 (pdf).
Hirokai Sai, Kwan Wee Tan, Kahyun Hur, Emily Asenath-Smith, Robert Hoven, Yi Jiang, Mark Riccio, David A. Muller, Veit Elser, Lara A. Estroff, Sol M. Gruner, Ulrich Wiesner. Hierarchical porous polymer scaffolds from block copolymers. Science  341 (2013) 530 - 534. (link).
H.T. Philipp, K. Ayyer, M.W. Tate, V. Elser, S.M. Gruner. Recovering structure from many low-information 2-D images of randomly selected samples. Journal of Physics: Conference Series. 425 (2013) 192016 (pdf).
Katherine S. Green, Marian Szebenyi, Kasey Boggs, Richard Bredthauer, Mark W. Tate, Sol M. Gruner. A prototype direct-detection CCD for protein crystallography. J. Appl. Crystallography 46 (2013) 1038-1048 (pdf).
Teeraporn Suteewong, Hirokai Sai, Robert Hoven, David Muller, Michelle Bradbury, Sol M. Gruner, Ulrich Wiesner (2013). Multicompartment mesoporous silica nanoparticles with branched shapes: an epitaxial growth mechanism. Science 340 (2013) 337-341 (link). 
Robin Baur, Mark W. Tate, Darren S. Dale, Sol M. Gruner. A high-spatial-resolution fiber-optic-coupled CMOS imager with novel scintillator for high-energy x-ray applications. Journal of Physics: Conference Series. 425 (2013) 062012 (pdf)
Katherine S. Green, Hugh T. Philipp, Mark W. Tate, Joel T. Weiss, Sol M. Gruner. Calibration and post-processing for photon-integrating pixel array detectors. Journal of Physics: Conference Series. 425 (2013) 062009 (pdf).
M.W. Tate, D. Chamberlain, K.S. Green, H.T. Philipp, P. Purohit, C. Strohman, S.M. Gruner. A medium-format, mixed-mode pixel array detector for kilohertz x-ray imaging. Journal of Physics: Conference Series. 425 (2013) 062004  (pdf).
Xin Liu, Kyoung-Su Im, Yujie Wang, Jin Wang, Mark W. Tate, Alper Ercan, Dniel R. Schuette, Sol M. Gruner (2007). Ultrafast and quantitative x-tomography and simulation of hollow-cone gasoline direct-injection sprays. SAE Int. J. Fuels Lubr. 116 : 85-91. Also DOE Report # ANL/XSD/58353. Also SAE Technical paper 2007-01-1847. DOI: 10.4271/2007-01-1847.
Sol M. Gruner. Imaging x-ray detectors open new vistas. Physics Today. (2012) 65, 29-34. (pdf).
Chae Un Kim, Jennifer L. Wierman, Richard Gillilan, Enju Lima, Sol M. Gruner. A high-pressure cryocoling method for protein crystals and biological samples with reduced background scatter. J. Appl. Cryst. (2013) 46, 234-241 (pdf).
Dayne West, Chae Un Kim, Chingkuang Tu, Jim Gordon, Arthur H. Robbins, Sol M. Gruner, David N. Silverman, Robert McKenna. Structural and kinetic effects on changes in the CO2 binding pocket of human carbonic anhydrase II. Biochemistry (2012) 51, 9156-9163. (link).
Marianne S. Hromalik, Katherine S. Green, Hugh T. Philipp, Mark W. Tate, Sol M. Gruner.  The FPGA Pixel Array Detector. Nucl. Instr. Meth. Phys. A (2012), 701, 7-16. (pdf).
Teeraporn Suteewong, Hiroaki Sai, Michelle Bradbury, Lara A. Estroff, Sol M. Gruner and Ulrich Wiesner.  Synthesis and Formation Mechanism of Aminated Mesoporous Silica Nanoparticles. Chem. of Materials (2012) 24, 3895-3905. (link).
Sebastien Boutet et al. High-resolution protein structure determination by serial femtosecond cyrstallography. Science (2012), 337, 362-364. (pdf).
Hugh T. Philipp, Kartik Ayyer, Mark W. Tate, Veit Elser, Sol M. Gruner. Solving structure with sparse randomly-oriented x-ray data. Optics Express(2012), 20, 13129-13137. (pdf), (movie 3MB).
Eric R. Meshot, Eric A. Verploegen, Mostafa Bedewy, Sameh Tawfick, Arthur A. Woll, Katharine S. Green,. Marianne Hromalik, Lucas J. Koerner, Hugh T. Philipp. Mark W. Tate, Sol M. Gruner, A. John Hart. High-speed in-situ x-ray scattering of carbon film nucleation and self-organization. ACS Nano (2012) 6, 5091-5101 ( link).
Suntao Wang, Mark Tate, Sol M. Gruner.  Protein crowding impedes pressure-induced unfolding of staphlococcal nuclease. Biochim. Biophys. Acta (2012) 1820, 957-961. (link).     

Suntao Wang, Yu-fei Meng, Nozomi Ando, Mark Tate, Szczesny Krasnicki, Chih-shiue Yan, Qi Liang, Joseph Lai, Ho-kwang Mao, Sol M. Gruner and Russell J. Hemley. Single-crystal CVD diamonds as small-angle X-ray scattering windows for high pressure research. J. Appl. Cryst. (2012) 45, 453-457. (pdf).  (Supplement1), (Supplement2).

Darren Dale, Sol M. Gruner, Joel Brock, Don Bilderback, Ernie Fontes. Science at the hard x-ray diffraction limint (XDL2011), Part I. Synchrotron Radiation News (2011) 24, 4-12. (link).
Morgan Stefik, Suntao Wang, Robert Hovden, Hiroaki Sai, Mark Tate, David Muller, Ullrich Steiner, Sol Gruner, Ulrich Wiesner.  Networked and chiral nanocomposites from ABC triblock terpolymer coassembly with transition metal oxide nanoparticles. J. Materials Chem. (2012) 22, 1078-1087. (link)
Chae Un Kim, Mark W. Tate, and Sol M. Gruner.  Protein Dynamical Transition at 110 K. Proc. Natl. Acad. Sci. USA (2011) 108, 20897-20901. (pdf).
Hugh T. Philipp, Mark W.Tate, Sol M. Gruner. Low-flux measurments with Cornell's LCLS integrating pixel array detector. JINST (2011) 6, C11006. (link).
Marcus D. Collins, Chae Un Kim, Sol M. Gruner. High-pressure protein crystallography and NMR to explore protein conformations. Annu. Rev. Biophysics. (2011) 40, 81-98 + Erratum (pdf).
Stephen T. Kelly, Jonathan C. Trenkle, Lucas J. Koerner, Sara C. Barron, Noel Walker, Philippe O. Pouliquen, Mark W. Tate, Sol M. Gruner, Eric M. Dufresne, Timothy P. Weihs and Todd C. Hufnage.  Fast x-ray microdiffraction techniques for studying irreversible transformations in materials. J. Synchrotron Radiation (2011) 18, 464-474. (pdf).
Ulrich Englich, Irina Kriksunov, Richard A. Cerione, Michael J. Cook, Richard Gillilan, Sol M. Gruner, Quingqui Huang, Chae Un Kim, William Miller, Soren Nielsen, David Schuller, Scott Smith, Doletha M.E. Szebenyi. Microcrystallography, high-pressure cryocooling and BioSAXS at MacCHESS.  J. Synchrotron Radiation (2010) 18, 70-73. (pdf).
Donald H. Bilderback, Georg Hoffstaetter, Sol M. Gruner. R&D toward an Energy Recovery Linac at Synchrotron Light Source. Synchrotron Radiation news. (2010) 23, 32-41. (pdf).
Morgan Stefik, Surbhi Mahajan, Hiroaki Sai, Thomas H. Epps III, Frank S. Bates, Sol M. Gruner, Ulrich Wiesner. Networked nanocomposites derived from block copolymers. Abstr. of Papers of the ACS, Aug 2010, San Francisco, CA. PSME Preprints. (2010). (pdf).
Ernest Fontes, Donald H. Bilderback, Sol M. Gruner. Status of CHESS facility and research programs: 2010. Nucl. Instr. Meth. Phys Res. A. (2011) 649, 3-5. (pdf).
Hugh T. Philipp, Marianne Hromalik, Mark Tate, Lucas Koerner, Sol M. Gruner. Pixel array detector for x-ray free electron laser experiments. Nucl. Instr. Meth. Phys Res. A. (2011) 649, 67-69. (pdf).
Teeraporn Suteewong, Hiroaki Sai, Roy Cohen, Suntao Wang, Michelle Bradbury, Barbara Baird, Sol M. Gruner, Ulrich Wiesner. Highly aminated mesoporous silica nanoparticles with cubic pore structure. J Amer. Chem. Soc. (2011) 133, 172-175 (link to paper), .
Lucas J. Koerner, Richard E. Gillilan, Katharine S. Green, Sunato Wang, Sol M. Gruner. Small angle solution scattering using the mixed-mode pixel array detector. J. Synchrotron Radiation. (2011) 18, 148-156 (.pdf 597k).
Lucas J. Koerner, Sol M. Gruner. X-ray analog pixel array detectors for single bunch time-resolved imaging. J. Synchrotron Radiation. (2011) 18, 157 - 164. (.pdf 803k).
F. Loehl, I. Bazarov, S. Belomestnykh, M. Billing, E. Chojnacki, Z. Conway, J. Dobbins, B. Dunham, R. Ehrlich, M. Forster, S.M. Gruner, C. Gulliford, G. Hoffstaetter, V. Kostroun, M. Liepe, Y. Li, X. Liu, H. Padamsee, D. Rice, V. Shemelin, E. Smith, K. Smolenski, M. Tigner, V. Veshcherevich, Z. Zhao. High current and high brightness electron sources. Proc. IPAC'10 (Kyoto, Japan, 23-28 May, 2010). (pdf 4.5 MB).
Teeaporn Suteewong, Hiroaki Sai, Jinwoo Lee, Michelle Bradbury, Taeghwan Hyeon, Sol M. Gruner, Ulrich Wiesner. Ordered mesoporous silica nanoparticles with and without embedded iron oxide nanoparticles: structure evolution during synthesis. J. Materials Chem. (2010) 20, 7807-7814. (.